Filter press

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Filter press

Filter press is a separation process, specially employed by solid/liquid separation using the principle of pressure drive, provided by a slurry pump. Filter press is a fixed volume and batch operation, which simply means that the operation must be stopped to discharge the filter cake before the next batch can be started.[1] The major components of filter press are skeleton and filter pack. The skeleton holds the filter pack together while pressure is being developed inside filter chamber. It however can only hold a specific volume of solids.

Concept Behind Filter Press Technology[edit]

Generally, the slurry needed to be dewatered is injected into the center of the press and fill up each chamber.[2] The filling time should be as quick as possible in order to avoid cake formation in the first chamber before filling up the last chamber. While the chambers are being filled up, the pressure inside the system will increase due to the formation of thick sludge.[3] Then, the liquid is filtered out through the filter clothes by adding streams of compressed air or water. The use of pressurized water require more time to pass into the chamber compared to pressurized air, however this method is much more cost efficient.

History[edit]

The first form of filter press was invented in British in 1853, used in obtaining seed oil through the use of pressure cells. However, there were many disadvantages associated with them, such as high labour requirement and discontinuous process. Major developments in filter press technology started in the middle of 20th century. In 1959, K. Kurita and S. Suwa succeeded in developing the world’s first automatic horizontal-type filter press to improve the cake removal efficiency, and moisture absorption. Nine years later, Kurita Company began developing flexible diaphragms to decrease moisture in filter cakes. The device enables optimisation of the automatic filtration cycle, cake compression, cake discharge and filter-cloth washing leading to the increment in opportunities for various industrial applications [4]

Types of Filter Presses[edit]

There are three main basic types of filter presses: Plate and Frame filter press, Recessed plate and frame filter press and Automatic filter press.

Plate and frame filter press[edit]

Plate and frame filter press is the most fundamental design among all the other filter presses, and majority nowadays refer it as “membrane filter plate”. This type of filter press consists of many plates and frames assembled alternately with the supports of a pair of rails. Presence of a centrifuge pump would ensure the remaining suspended solids do not settle in the system and its main function is to deliver the suspension into each of the separating chambers in the plate and frame filter. For each of the individual separating chambers, there is one hollow filter frame separated from two filter plates by filter clothes. The introduced slurry flows through a port in each individual frame, and the filter cakes are accumulated in each the hollow frame. As the filter cake becoming thicker, the filter resistance increases as well. So when the separating chamber is full, the filtration process is stopped as the optimum pressure difference had reached. The filtrate that passes through filter cloth are collected through collection pipes and stored in the filter tank. Whereas filter cakes (suspended solids) accumulation occurs at the hollow plate frame, then being separated at the filter plates by pulling the plate and frame filter press apart. The cakes would just fall off from those plates and being discharge to the final collection point . [5]

Cake discharge can be done in many ways. For example: Shaking the plates while they are being opened or shaking the cloths. Scraper can also be used, by moving from one chamber to another and scrape the cake off the cloth. At the end of each run, the cloth are cleaned using wash liquid and ready to start the next cycle [6]

Automatic Filter Press[edit]

Automatic filter press has the same concept as the manual filter and frame filter just that the whole process is fully automated. It consists of larger plates and frames filter presses with mechanical “plate shifter”.[4] The function of the plate shifter is to move the plates and allow rapid discharge of the filter cakes accumulated in between the plates. It also contains diaphragm compressor in the filter plates which aids in optimizing the operating condition by further drying the filter cakes.[4]

Recessed plate filter press[edit]

For recessed-plate filter press, it is made up of polypropylene squares at about 2 to 4 feet across with concave depression and a hole in the center.[7] Two plates join together to form a chamber to pressurize the slurry and squeeze the filtrate out through the filter cloth lining in the chamber.[7] It is capable of holding 12 to 80 plates adjacent to each other depending on the required capacity. When the filter press is closed, a series of chambers is formed. The differences with the plate and frame filter are that the plates are joined together in such a ways the cake recess on each plate, the cake thickness is restricted to 32mm unless extra frames are used which acts as spacers.[8] However there are disadvantages to this method such as longer cloth changing time, unable to accommodate filter papers as well as the possibility of forming uneven cake.[8]

Applications[edit]

Filter presses are used in a huge variety of different applications, from dewatering of mineral mining slurries to blood plasma purification.[6] At the same time, filter press technology is widely established for ultrafine coal dewatering as well as filtrate recovery in coal preparation plants. According to G.Prat [9] “filter press is proven to be the most effective and reliable technique to meet today’s requirement”. One of the examples is Pilot scale plate filter press, which is specialized in dewatering coal slurries. In 2013 the Society for Mining, Metallurgy and Exploration published an article highlighting this specific application.[9] It was mentioned that the use of filter press is very beneficial to plant operations since it offers dewatering ultraclean coal as product, as well as improving quality of water removed to be available for equipment cleaning.

Many specialized applications are associated with different types of filter press that are currently used in various industries. Plate filter press is extensively used in sugaring operations such as the production of maple syrup in Canada, since it offers very high efficiency and reliability. According to M.Isselhardt “appearance can affect the value of maple syrup and customer's perception of quality”.[10] This makes the raw syrup filtration process extremely crucial in achieving desired product with high quality and appealing form, which again suggested how highly appreciated filter press methods are in industry.

The detailed applications in food industry,mining industry,pharmaceutical industri,chemical industry, wastewater treatment etc. are as follows:[11]

1, Chemical industry: dyes, pesticides, silicic acid, glycerin, white carbon, busy, sodium carbonate, additives, basic chemicals, chemical filler, pigment, white alumina, manganese, caustic soda, soda ash, alkali salts mud, saponin, graphite, bleaching powder, Synaptic powder phosphor, sodium hydrosulfite, potassium chlorate, potassium sulfate, ferrous sulfate, ferric hydroxide, water purification agent ( aluminum sulfate, chloride, basic aluminum chloride ) and so on,filter press is the ideal filtration equipment in these applications ; 2, Food industry : wine filter press, yeast, fruit juice filter press, edible oil, vegetable oil, soy sauce, sugar mills, rice wine, white wine, fruit juices, soft drinks, beer, yeast, citric acid, vegetable protein, plant density sweetener, glucose, stevioside, maltose, starch, rice flour, corn syrup, gum, carrageenan, monosodium glutamate, spices, butter, oral liquid, soy, seaweed ; 3, Metallurgical industry : gold, platinum, uranium, cobalt, nickel, zinc, manganese, copper, iron sands filter press ; 4, Non-metallic minerals : tailings, coal, acid clay, bentonite, kaolin, ceramics, cement, clay, industrial sand ; 5, Pharmaceutical industry : enzymes, amino acids, antibiotics, pharmaceutical intermediates, bulk drugs, medicine, blood products, antibiotics ( chlortetracycline, erythromycin, spiramycin, Jinggangmeisu, Midecamycin, tetracycline, berberine, oxytetracycline ), calcium phytate, Chinese inositol, growth derived sand, organic phosphorus, glucoamylase ; 6, Environmental Engineering : Chemical waste water, wastewater filter press, mining wastewater filter press, domestic wastewater, waste water, waste steel, waste removal, leather wastewater, ports silt, mud, salt mud wastewater, carbide slag, gypsum, waste acid recovery, gold clarification of liquids mine tailings, biological wastewater, wastewater, sewage smelting, printing and dyeing wastewater, sewage brewing, pharmaceutical waste water, sewage and other environmental particulates, new equipment purification process. 7, Refining : white oil, sesame oil, light oil, glycerin, mechanical oil, vegetable oil. 8, clay industry : kaolin, bentonite, activated clay, clay, electronic ceramics clay. 9, the automotive industry : filtration, decorative

Main Process Characteristics[edit]

Table 1 Classification of filter press.[12]

Specifications Parameters Units
Scale 1-100 m3/hr
Operation Batch, Continuous
Objectives Clarification, Solids Recovery
Slurry settling characteristics
Rate <0.1 to >5 cm/s
Clarification Poor
Proportion of sludge < 2% vol to > 20% vol
Slurry filtering characteristics Slow at the rate of cm/h, up to 10 hr

Feed[edit]

Typical range of particle size and feed concentration are 1-100 μm and 1-30% by weight.[13] The slurry feed concentration generally has large amount of ultrafine particles. The percentage of solids concentration in the slurry feed is normally more than 10% by weight.[9]

Operation[edit]

Whereas limitation in pressure resistance of the filter cake is up to a maximum of 800 kPa.[13] Flow rate of filtrate is controlled by feed pump. In filter press methodology, positive pressure filtration is used instead of vacuum filtration with high-energy consumption.[5][14]

Efficiency[edit]

Plate and frame filter press produce up to 99% of solids recovery and the moisture left in the cake is commonly ranging from 15% to 20%.[9] During cake washing, 90% of the filtrate can be removed by the wash liquid.[15]

Assessment of important characteristics[edit]

Here are some typical filter press calculation used for handling operation applied in waste water treatment

Solids loading rate[edit]

S=(B x 8.34 lb/gal x s)A
Where,

S is the solid loadings rate in lbhr.
B is biosolids in galhr
s is the % solids/ 100.
A is the plate area in ft2.

Net filter yield[edit]

NFY = S × P / TCT
Where,

NFY  is the net filter yield in lb/hr/ ft2. 
S is the solids loadings rate in lb/hr/ ft2.
P is the period in hr.
TCT is the total cycle time in hr.

(S × P) gives the filter run time.[16]

Flow rate of filtrate[edit]

u=(1A)dV/dt=∆P[μ(R_c+R_f )]

Where:

u is flow rate of filtrate through cloth and cake (m/s), dV/dt is volumetric filtration rate (m3/s), is the resistance of the filter cake (m-1), is the initial resistance of the filter (resistance of an initial layer of cake, filter cloths, plate and channel) (m-1), is the viscosity of the filtrate (N·s/m2), is the applied pressure difference (N/m2) one side to another side of the filter medium, A is the filtration area (m2). Those are the most important factors that affect the rate of filtration. When filtrate pass through the filter plate, deposition of solids are formed and increases the cake thickness, which also increase Rc while Rf is assumed to be constant.[17] The flow resistance from cake and filter medium can be studied by calculating the flow rate of filtration through them.

If the flow rate is constant, the relationship between pressure and time can be obtained. The filtration must be operated by increasing pressure difference to cope with the increase in flow resistance resulting from pore clogging.[17] The filtration rate is mainly affected by viscosity of the filtrate as well as resistance of the filter plate and cake.

Optimum time cycle[edit]

High filtration rate can be obtained from producing thin cake. However, conventional filter press is a batch system and the process must be stopped to discharge the filter cake and reassemble the press, therefore this operation is time consuming. Practically, maximum filtration rate is obtained when the filtration time is greater than the time taken to discharge the cake and reassemble the press to allow for cloth’s resistance.[17] Properties of filter cake affect the filtration rate and it is desirable for the particle’s size to be as large as possible to prevent pore blockage by using coagulant. From experimental work, flow rate of liquid through the filter medium is proportional to the pressure difference.[15] As the cake layer forms, pressure applies to the system increases and the flow rate of filtrate decreases.[8] If the solid is desired, the purity of the solid can be increased by cake washing and air drying.[12] Sample of filter cake can be taken from different locations and weighed to determine the moisture content by using overall material balance.[9]

Possible heuristics to be used during design of the process[edit]

The selecting of filter press type depends on the value of liquid phase or the solid phase. If extracting liquid phase is desired, then filter press is among the most appropriate methods to be used.[18]

Materials[edit]

Nowadays, filter plates are made from polymers or steel coated with polymer. They give good drainage surface for filter cloths. The plate sizes are ranged from 10 by 10 cm to 2.4 by 2.4 m and 0.3 to 20 cm for the frame thickness.[12]

Filter medium[edit]

Typical cloth areas are range from 50 to 1000 m2, even though plates can provide filter areas up to 2000 m2. Normally, plate and frame filter press can form up to 50 mm of cake thickness, however, it can be push up to 200 mm for extreme cases. Recessed plate press can form up to 32 mm of cake thickness.[8]

Operating condition[edit]

The operating pressure is commonly up to 7 bars for metal.[12] The improvement of the technology makes it possible to remove large amount of moisture at 16 bar of pressure and operate at 30 bars.[6] However, the pressure is 4-5 bars for wood or plastic frames.[12] If the concentration of solids in the feed tank increase until the solid particles are attached to each other. It is possible to install moving blades in the filter press to reduce resistance to flow of liquid through the slurry.[14] For the process prior to cake discharge, air blowing is used for cakes that have permeability of 10−11 to 10−15 m2.[9]

Pre-treatment[edit]

Pre-treatment of the slurries before filtration is required if the solid suspension has settled down. Coagulation as pre-treatment can improve the performance of filter press because it increases the porosity of the filter cake leading to faster filtration. Varying the temperature, concentration and pH can control the size of the flocs. Moreover, if the filter cake is impermeable and difficult for the flow of filtrate, filter aid chemical can be added to the pre-treatment process to increase the porosity of the cake, reduce the cake resistance and obtain thicker cake. However, filter aids need to be able to remove from the filter cake either by physical or chemical treatment. A common filter aid is Kieselguhr, which give 0.85 voidage.[14]

In terms of cake handling, batch filter press requires large discharge tray size in order to contain large amount of cake and the system is more expensive compare to continuous filter press with the same output.[6]

Production of waste stream - Post-treatment[edit]

Washing[edit]

There are two possible methods of washing that are being employed, the “simple washing” and the “thorough washing”. For simple washing, the wash liquor flows through the same channel as the slurry with high velocity causes erosion of the cakes near the point of entry. Thus the channels formed are constantly enlarged and therefore uneven cleaning is normally obtained. A better technique is by thorough washing in which the wash liquor is introduced through a different channel behind the filter cloth called washing plates. It flows through the whole thickness of the cakes in opposite direction first and then with the same direction as the filtrate. The wash liquor is normally discharge through the same channel as the filtrate. After washing, the cakes can be easily removed by supplying compressed air to remove the excess liquid.[12]

Waste[edit]

Nowadays filter presses are widely used in many industries, they would also produce different types of wastes. Harmful wastes such as toxic chemical from dye industries, as well as pathogen from waste stream might accumulate in the waste cakes; hence the requirement for treating those wastes would be different. Therefore before discharge waste stream into the environment, application of post-treatment would be an important disinfection stage. It is to prevent health risks to the local population and the workers that are dealing with the waste (filter cakes) as well as preventing negative impacts to our ecosystem. Since filter press would produce large amount of waste, if it was to be disposed by land reclamation, it is recommended to dispose to the areas that are drastically altered like mining areas where development and fixation of vegetation are not possible. Another method is by incineration, which would destroy the organic pollutants and decrease the mass of the waste. It is usually done in a closed device by using a controlled flame.[5]

Advantages and Disadvantages Compared to other Competitive Methods[edit]

Many debates have been discussed about whether or not filter presses are sufficient to compete with modern equipment in present time as well as the upcoming years, since filter presses were among one of the oldest machine-driven dewatering devices. There are many applications where modern filter presses have the best characteristics for the job, where efficiency improvements are possible. However throughout the years, despite the fact that many mechanical improvements have been made, filter presses still remain to operate on the same concept as when it was first invented, poor progress on efficiency improvement as well as lack of research on conquering associated issues surrounding filter presses have suggested a possibility of performance inadequacy. At the same time, many other filters could do the same job as filter presses deliver or even better. In certain cases, it is crucial to compare characteristics and performances.[19]

Batch Filter Press versus a Continuous Vacuum Belt Filter[edit]

Filter presses offer a wide range of application, one of its main propositions is the ability to provide a large filter area in a relatively small footmark. Surface area available is one of the most important dimensions in any filtering process, since it maximises filter flow rate and capacity. A standard size filter press offers a filter area of 216 m2, whereas a standard belt filter only offers approximately 15 m2.[19]

High-Solids Slurries: Continuous Pressure Operation[edit]

Filter presses are commonly used to dewater high-solids slurries in metal processing plants, one of the press filter technology that could deliver the job is the Rotary Pressure Filter method, which provides continuous production in a single unit, where filtration is directed via pressure. However in cases where solids concentration in high-solids slurries is too high (50%+), it is better to handle these slurries using vacuum filtration, such as a continuous Indexing Vacuum Belt Filter, since high concentration of solids in slurries will increase pressure and if pressure is too high, the equipment might be damaged and/or less efficient operation.[19]

Current development[edit]

In the future, market demands for modern filtration industry are going to become finer and higher degree in separation, and particularly on the purpose of material recycling, energy saving, and green technology. In order to meet increasing demands for higher degree of dewatering from difficult-to-filter material, super-high pressure filters are required. Therefore the trend in increasing the pressure for the automatic filter press will keep on developing in the future.

The conventional filter press mechanisms usually use mechanical compression and air to de-liquoring; however, the efficiency of producing low-moisture cake is limited. An alternative method has been introduced by using steam instead of air for cake dewatering. Steam dewatering technique can be a competitive method since it offers product of low-moisture cake.[20]

examples of Filter Presses in use at

flowpress.net

References[edit]

  1. ^ "What is a filter press?". 
  2. ^ [:http://www.micronicsinc.com/technical-data/faq/ "SIEMENS. 2011. What is a Filter Press?"]. 
  3. ^ [:http://www.lenntech.com/library/sludge/presses/filter-press.htm "Filter presses for sludge treatment"]. LENNTECH. Retrieved 09/10/2013. 
  4. ^ a b c Shirato, M. "Filter press: A review of development in automatic filter presses". filtsep. Retrieved 05/10/13. 
  5. ^ a b c Von Sperling, M. Biological Wastewater Treatment: Wastewater Characteristics Treatment and Disposal. IWA PUBLISHING. Retrieved 06/10/13. 
  6. ^ a b c d SUTHERLAND, K (2008). Filters and Filtration Handbook (5th edition). Elsevier. 
  7. ^ a b EPA. "Biosolids technology fact sheet : Recessed-plate filter press, washington, D.C.". Retrieved 05/10/13. 
  8. ^ a b c d TARLETON, E. S. W., R. J (2007). Solid/liquid separation - equipment selection and process design,. Elsevier. ISBN 978-0-080-46717-7. 
  9. ^ a b c d e f Chanllenges in Fine Coal Processing, Dewatering, and Disposal chapter 10. Society for Mining, Metallurgy, and Exploration (SME). 2012. ISBN 978-1-62198-038-4. 
  10. ^ "Recommendation for proper plate filter press operation, Filter press". PROCTOR MAPLE RESEARCH CENTER. 
  11. ^ [:http://www.press-filter.com/faq/filter-press-applications-05.html "Filter press applications"]. lingduxiaolang. Retrieved 05/04/2014. 
  12. ^ a b c d e f Perry’s Chemical Engineer’s Handbook (8th Edition). 2008. pp. 2022, 2036, 2023. 
  13. ^ a b TARLETON, E. S. W., R. J (2007). Solid/liquid separation - equipment selection and process design,. Elsevier. ISBN 978-0-080-46717-7. 
  14. ^ a b c CHEREMISINOFF, N. P. (1998). Liquid Filtration (2nd Edition). Elsevier. ISBN 978-0-0805-1036-1. 
  15. ^ a b J H HARKER, J. R. B., J.F. RICHARDSON. Coulson & Richardson Chemical Engineering Particle Technology & Separation Processes. Oxford, Butterworth-Heinemann. ISBN 0750644451. 
  16. ^ F.R. Spellman (2008). Handbook of water and waste water treatment plant operations, (second edition). 
  17. ^ a b c CHEREMISINOFF, N. P (1998). Liquid Filtration (2nd Edition). Elsevier. ISBN 978-0-0805-1036-1. 
  18. ^ ALEJANDRO ANAYA DURAND; JOSSELINE ALARID MIGUEL; GABRIEL GALLEGOS DIEZ BARROSO; LEON GARCIA, M. A. J. P. S. A. (2006). Heuristics Rules for Process Equipment. Chemical Engineering. pp. 113, 44–47. 
  19. ^ a b c PERLMUTTER, B. "A REVIEW OF FILTER PRESS BASICS AND ISSUES VERSUS ALTERNATIVE BATCH OR CONTINUOUS REPLACEMENT TECHNOLOGIES". 
  20. ^ Teemu Kinnarinen; Antti Häkkinen & Bjarne Ekberg (2013). Steam Dewatering of Filter Cakes in a Vertical Filter Press, Drying Technology: 31:10, 1160–1169. doi:10.1080/07373937.2013.780246.