Fisher-Porter tube
A Fisher-Porter tube or Fisher-Porter vessel is a glass pressure vessel used in the chemical laboratory. The reaction vessel consists of a lipped heavy-wall borosilicate glass tube and a lid made from stainless steel. The lid is sealed with an o-ring and held in place with a coupling.
The advantage over steel autoclaves is that the progress of a reaction can be followed by eye. The maximum pressure that can be achieved is much lower than that in a metal bomb. For example, typical pressure ratings are 7 bar for a large 335 mL Fisher-Porter vessel and 15 bar for a small 90 mL one, whereas the usual kind of bomb is safe to use with 200 bar. Illustrative applications involve reactions at elevated temperatures using volatile reagents.[1]
Name
The name has become something of a genericised trademark. For decades these flasks used to be made by the Fisher & Porter Company until it became a part of ABB. Nowadays they are sold by Andrews Glass under the Lab-Crest label.
Alternatives
Ace Glass offers thick-walled glass tubes with their proprietary Ace-Thred screw caps. Caps are available to fit gas plunger valves to admit gases under pressure. Similar arrangements are available from Q Labtech and sold through Sigma-Aldrich.
External links
References
- ^ "Telomerization of Isoprene with Dialkylamine: N,N-Diethylnerylamine". Org. Synth. 67: 48. 1989. doi:10.15227/orgsyn.067.0048.
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